2 x 15 Liter Supercritical Fluid System

2 x 15 Liter Supercritical Fluid System

(1 đánh giá)

2x15 liter

Applied Separations

12 Months

2 x 15 Liter Supercritical Fluid System - Applied Separations, Inc.

TECHNICAL SPECIFICATIONS
 
System Recirculating Cooling Bath (RCB):
 
•  10 Tons of Cooling Capacity
Circulates water/inhibited glycol mix. (Water & Glycol mixture supplied by customer on-site.)
•   Rated to -5°C
 
CO2 Pumping module:
 
•  Pneumatic CO2 pump
•   Delivers up to 3 kg of CO2/min. at 690 Bar (10,000 psi) max*
*based on incompressible liquid
•   Cooled by the system recirculating cooling bath
•   Powered by customer-supplied compressed air source
 
Extraction Modules:
 
•  Two (2) stainless steel, 15-liter vessels
•   690 Bar (10,000 psi) maximum operating pressure
•   100° C maximum operating temperature
•   Threaded closure – no bolts to torque.
•   Heated with special electrical band heaters
Two (2) interior stainless-steel baskets for quick loading/unloading
Heated, automated flow metering valve controls outlet flow at outlet of each extraction vessel
 
Separation Module:
 
•  Separator for Extraction Vessel 1
•   One (1) stainless steel, heated, 4-liter cyclonic separator vessel
o Rated for 124 Bar (1,800 psi) at 100° C
o Pressure relief safety device installed
o Level Indicator
•   One (1) stainless steel, heated, 1-liter collection vessel
o Collects precipitated material from separator
o Rated for 124 Bar (1,800 psi) at 100° C
•   One (1) flow meter
•  Separator for Extraction Vessel 2
•   One (1) stainless steel, heated, 4-liter cyclonic separator vessel
o Rated for 124 Bar (1,800 psi) at 100° C
o Pressure relief safety device installed
o Level Indicator
•   One (1) stainless steel, heated, 1-liter collection vessel
o Collects precipitated material from separator
o Rated for 124 Bar (1,800 psi) at 100° C
•   One (1) flow meter
 
CO2 Recycling System:
 
•  One (1) CO2 condenser
•  One (1) 60 liter, stainless steel, CO2 storage vessel
o Rated for 113 Bar (1,650 psi) at 100° C
o Pressure relief safety valves installed
 
Modifier/Liquid Pump:
•  High-pressure, pneumatic pump with cycle timer
o 400 mL/min maximum flow rate
 
Control, Monitoring:
 
•  Pressure control
•   Air pressure regulated to the pump
•   Monitored by an analog air pressure gauge
•   Digital CO2 pressure gauge
•  Temperature control
Heat exchanger provides heating for the supercritical fluid before entering the vessel
•   Vessel temperature is maintained with a PID controller
 
•  Flow Control
Heated, automated flow control valve on each extraction vessel outlet.
•   Flow rate set and monitored on HMI
 
•  Control / Monitoring
•   Windows-based, Touch screen PC with LabVIEW-based ASI Vision
software interface controls and/or monitors critical system variables
All PID controllers have RS-485 outputs for extensive data logging through software
•   Local pressure indicators
•   Local flow indicators
 
Valves and Fittings:
 
•  All 10,000 psi (690 Bar) rated
 
 
 
 
 
 
 
Modular System Frame:
 
 
•  Welded/bolted heavy gauge steel construction
•  Caster-mounted for easy repositioning
High performance, chemical-resistant, polymer coating to minimize corrosion
Integrated lifting boom and electric winch to simplify loading/unloading of product baskets
 
Documentation:
 
 
At time of delivery, an operator’s manual will be included with full details
covering:
•  Instructions as to the principles of SFE
•  Scope, purpose and operating parameters of the system
•  Set up (utilities, assembly) installation and startup
•  Instrument set up and instruction
•  Operation, care and maintenance
•  Troubleshooting

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