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Supercritical Fluid Systems
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1 x 100L Liter Supercritical Fluid System
SFC
Applied Separations
12 months
Applied Separations, Inc. offers SCF systems in any size and configuration. Although the size of a pilot system versus a production system is arbitrary, customarily, Applied Separations designates pilot systems as having extraction/reaction vessels from 5 liters to 100 liters. Greater than 80 liters, we consider production scale.
1 x 100L Liter Supercritical Fluid System
TECHNICAL SPECIFICATIONS
System Recirculating Cooling Bath (RCB):
• 10 Tons of Cooling Capacity
• Circulates water/inhibited glycol mix
• Rated to -10°C
CO2 Pumping module:
• Electric-powered, Hydraulic CO2 pump
• Delivers up to 6kg of CO2/min. at 690 Bar (10,000 psi) max
• Pump heads cooled by the system recirculating cooling bath
Extraction Module:
• One (1) stainless steel, 100 liter vessel
• Manufactured using applicable ASME guidelines. Specific ASME or other vessel certification available for an additional fee.
• 690 Bar (10,000 psi) maximum operating pressure
• 100° C maximum operating temperature
• Patented Emergency Pressure Relief Device (see Addendum A)
• Breach lock-style closure
• Heated with special flexible electrical heaters
• CO2 inlet line in vessel sidewall to simplify opening and closing
• One (1) interior stainless steel basket for quick loading/unloading
• Automatic flow controlling valve between extraction vessel and separator.
Separation Module:
• Separator
• One (1) stainless steel, heated, 15 liter cyclonic separator vessel
o Rated for 124 Bar (1,800 psi) at 100° C
o Manufactured using applicable ASME guidelines. Specific ASME
or other vessel certification available for an additional fee.
o Pressure relief safety device installed
o Level Indicator
• One (1) stainless steel, 4 liter collection vessel
o Collects precipitated material from separator
o Rated for 124 Bar (1,800 psi) at 100° C
o Manufactured using applicable ASME guidelines. Specific ASME
or other vessel certification available for an additional fee.
• Flow meter
CO2 Recirculation System:
• One (1) CO2 condenser
• Stainless steel, CO2 storage vessels
o 200L of total storage capacity
o Rated for 113 Bar (1,650 psi) at 100° C
o Manufactured using applicable ASME guidelines. Specific ASME
or other vessel certification available for an additional fee.
o Pressure relief safety valve installed
Control, Monitoring:
• Pressure control
• Hydraulic pressure regulator
• Monitored by an analog pressure gauge
• Digital CO2 pressure gauge
• Temperature control
• Heat exchanger provides heating for the supercritical fluid before entering the vessel
• Vessel temperature is maintained with a PID controller
• Flow Control
• Heated auto-flow control valve between extraction vessel and separator vessel.
• Flow rate monitored on HMI
• Control / Monitoring
• Windows-based, Touch screen PC with LabVIEW-based ASI Vision software interface controls and/or monitors critical system variables
• All PID controllers have RS-485 outputs for extensive data logging through software
• Local pressure indicators
• Local flow indicators
Valve and Fittings:
• All 10,000 psi (690 Bar) rated and meet applicable ASTM standards, where appropriate.
Modular System Frame:
• Welded/bolted steel construction
• Caster-mounted for easy repositioning
• High performance, chemical-resistant, polymer coating to minimize corrosion
• Integrated pressure vessel lid lifting hoist with overhead boom
• Modification of standard system frame layout may incur an additional fee
Documentation:
An operator’s manual will be included with full details covering:
• Instructions as to the principles of SFE
• Scope, purpose and operating parameters of the system
• Set up (utilities, assembly) installation and startup
• Instrument set up and instruction
• Operation, care and maintenance
• Troubleshooting
• List of part numbers for consumable items and major components.
• Pressure vessel raw material certification, hydro-test certification, and design calculations, where applicable
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